Table 1 Detailed description of the operating conditions of the GC
Parameter | Value |
|---|---|
Injector temperature set point | 120 °C |
Injector flow rate | 21Â ml/min |
Type of column | Packed Column |
FFAP | 15% Chromosorb which is highly polar |
Column flow rate | 20Â ml/min |
Initial oven temperature | 60 °C on hold for 5 min |
Final oven temperature | 120 °C on hold for 5 min |
Temperature increases interval | at 10 °C/min interval |
Detector temperature | 250 °C |
Reference flow rate | 50Â ml |
Limit Of detection (Methanol) | 1.43 × 10−4%Vol |
Limit of detection (Ethanol) | 1.54 × 10−4%Vol |
Limit of quantification (Methanol) | 4.77 × 10−4%Vol |
Limit of quantification (Ethanol) | 5.12 × 10−4%Vol |
Recovery Range % | 80%–100% |