|
Injector temperature set point
|
120 °C
|
|
Injector flow rate
|
21 ml/min
|
|
Type of column
|
Packed Column
|
|
FFAP
|
15% Chromosorb which is highly polar
|
|
Column flow rate
|
20 ml/min
|
|
Initial oven temperature
|
60 °C on hold for 5 min
|
|
Final oven temperature
|
120 °C on hold for 5 min
|
|
Temperature increases interval
|
at 10 °C/min interval
|
|
Detector temperature
|
250 °C
|
|
Reference flow rate
|
50 ml
|
|
Limit Of detection (Methanol)
|
1.43 × 10−4%Vol
|
|
Limit of detection (Ethanol)
|
1.54 × 10−4%Vol
|
|
Limit of quantification (Methanol)
|
4.77 × 10−4%Vol
|
|
Limit of quantification (Ethanol)
|
5.12 × 10−4%Vol
|
|
Recovery Range %
|
80%–100%
|
